Apparatus and method for static sedimentation tests comprising a plurality of sedimentation cylinders, which are subject to the same mixing conditions

ABSTRACT

The invention relates to an apparatus for static sedimentation tests comprising a plurality of sedimentation cylinders, which are subject to the same mixing conditions, said apparatus comprises:
         a. A variable number of transparent sedimentation cylinders, the most common being 12;   b. Each sedimentation cylinder is located inside a non-intrusive emitter and receiving sensor housing where each housing has an electronic ID card, electronic circuit boards and connection to a control system;   c. A support structure containing the sedimentation cylinders and sensor housings which rotates around an axis of rotation;   d. Each sedimentation cylinder has a bottom stopper and top stopper;   e. Where each bottom stopper of each sedimentation cylinder is mounted on a lateral bar parallel to the rotation axis, by a fixing to the supporting structure;   f. Also the sedimentation cylinders are fixed in the supporting structure by a clamping system around the top stopper of each sedimentation cylinder   g. The top stopper of each sedimentation cylinder has an additive injection system.       

     In addition, its presented a method for static sedimentation tests carried out simultaneously and under the same mixing conditions in a plurality of sedimentation cylinders, the most common being 12; which rotate around an axis of rotation; where each sedimentation cylinder is located inside a sensor housing which are connected to a control system.

TECHNICAL FIELD

The proposed invention relates to the field of solid-liquid separationof slurries or pulps required in many small scale and large industrialprocessing applications, and looks for a total transformation of bothhow the separation tests are done and the method of collecting data andgenerating results, thanks to its control system. In addition to thefield of solid-liquid separation, the same invention can be used inliquid-liquid separation applications where dense media separationoccurs and can be determined through boundary condition identification.

The invention includes an apparatus for performing static sedimentationtests and a method for measuring sedimentation through staticsedimentation tests, incorporating digital sensors specially programmedfor this purpose, to obtain raw data and/or comparison parameters,generating the expected results.

PRIOR ART

Solid-Liquid Separation

Slurries, pulps or liquids with suspended particles are often requiredto have the suspended particles and process liquor (often referred to assupernatant liquid) separated. This process is often referred to asthickening or clarification and applies to multiple industries with thegoal of recovering either the process liquor (supernatant) or thesuspended particle material for reuse in the processing procedure,further processing, or disposal. During the thickening or clarificationprocess, a slurry or pulp is continuously fed into a thickener,clarifier or settling tank device, where the suspended particles areallowed to settle under the influence of gravity to form a thickened mudbed on the bottom of the tank or vessel. This mud is normally referredto as an underflow, is removed, normally by a pump at the base of thetank or vessel, and either processed or disposed of. The process liquor,with minimal suspended particles, is removed from the top of the tankand is either discharged, reused in the industrial process orreprocessed in another clarification tank for further solid-liquidseparation.

In a thickener, clarifier or settling tank, chemical products(principally, but not limited to, flocculants and coagulants) may bemixed with the slurry as it is fed into the tank. This is usuallyreferred to as the feed-well of the tank where mixing occurs between theslurry and the additive that promote gravity sedimentation of theparticles in the slurry to accumulate in the mud bed and be removed bythe underflow pump. The underflow extraction point is normally centrallylocated at the bottom of the tank and the base of the tank is normallyconical in shape incorporating a rake mechanism to push this thickenedmud towards the extraction point. This provides continuous operationswhereby thickened mud (underflow) and clarified liquor (overflow) areextracted while slurry to be treated (feed) is simultaneously mixed witha chemical additive and fed into the tank.

Liquid-Liquid Separation

The dense fraction separation of liquids is often required in manyprocess fields to refine or purify a particular product or material. Oilrefinery is a specific case whereby crude oil is separated into lighterfractions by the fractional distillation process. For this particularprocess, the density of the various extracted liquids, such as diesel,kerosene and gasoline vary and provide a form of distinguishing thisproperty through dense fraction separation. There are many varieties andtechniques of liquid-liquid separation specific to a particular processor methodology. Those whereby a boundary between different fractions canbe visually distinguished or through emitted wavelength propagationcharacteristics, can benefit from the use of the presented invention todetermine these boundary changes with time.

The invention is primarily targeted at the solid-liquid separationindustry, but can be equally applied to liquid-liquid separationprocesses.

Settling Tests

There are several types of settling tests, the most common is mixingslurries in sedimentation cylinders measuring the height of the solidsas the slurry settles.

Performing more than one sedimentation test simultaneously creates thechallenge of ensuring that all sedimentations tests are carried outunder the same condition and consequently, there are several solutionsthat now allow this. Particularly in the field of health, blood mixersare widely used, which consists of a machine containing tubes thatrotate around an axis in order to mix the contents of each tube.

For the specific case of inorganic sedimentations, in particular in thefield of mining, a similar system to the blood mixing system is used,except in the case of chilean patent CL43863, where two side bracketsare sustaining the axis, instead of one, as is often used in bloodmixers.

While at first glance the present invention may seem similar to theaforementioned Chilean patent, it presents substantial differences thatmake them distinct to each other.

In terms of form:

a. Patent CL43863 has two axes in the middle of horizontal plates (claim1.C.), while the present invention has one axis at a greater height, inorder to enable the apparatus to naturally return to the verticalposition without manual intervention or need of a peg as described inclaim 1.G. of said patent.b. Patent CL43863 specifies that the tubes are located inside the frame(claim 1.D.) while the present invention contemplates a new orientationof tubes, which are alternately located laterally outside the frame orsupport structure, thus to reduce size and optimize efficiency. This newfeature allows the use of many more tubes and is only possible becauseautomatic sensors are used for measurement instead of traditionaloptical methods. Also, it allows to have enough space to install thecontrol system and electronic parts, which is new with regard to whatwas presented in the chilean patent.c. Patent CL43863 specifies from 1 to 10 tubes (claim 1.D.) while thepresent invention is designed for a variable number of tubes, the mostcommon being 12, since in this way the new method of mixing allowsmeasurement methods by using automatic sensors and not traditionaloptical methods, giving reliable results.d. Patent CL43863 considers a crank (1.D.), while the present inventiondoes not have this manual mechanism, since it considers anelectro-mechanical mechanism programmed according to the desiredresults.e. The proposed invention has housings that cover and/or surround eachof the tubes/sedimentation cylinders and the measurement sensors, whilePatent CL43863 has no housings since that it does not consider sensorsand its associated measurement methodology.f. In Patent CL43863 sedimentation occurs by gravity, while in thepresent invention, the system has a dosing device, which encouragessedimentation by supplying flocculants in the same apparatus.

In terms of substance:

Patent CL43863 discloses an instrument for doing simultaneous slurriessettling tests, not including a method nor instruments for alsomeasuring transparency of the liquid. In other words, the procedures andtest methods are preserved intact. The present invention relates to atotal transformation of both the manner in which the tests are conductedand the method in which data are collected through a custom program thatgenerates immediate, computerized and reliable results by not havinghandling and manual interpretation. Given these characteristics, thedifferences mentioned are important and completely necessary to achievethe objective of this invention.

Chemical Additives

The principal chemical additives used in solid-liquid separation includeflocculants, coagulants and ph-modifiers. Flocculants and coagulants areprovided by many global chemical companies and often consist of apolymer molecular structure which agglomerates with suspended particlesin a slurry to form flocculant chain structures, commonly referred to asflocs. These chains of particles settle faster than if the particleswere separated and therefore increase the settling rate of the slurrywithin the thickener, clarifier or settling tank.

The properties of slurries and pulps are highly variable between processoperations, and hence there are many types and combinations offlocculants and coagulants available on the market. Principally themolecular weight of the additive is varied, the charge, pH, unit costand the physical form.

The performance of each type of additive is affected principally by thedilution of the slurry feed, the chemistry of the slurry (including, butnot limited to, pH and oxidation-reduction potential), the dilution orpreparation of the additive, and the dosage. For the thickener,clarifier and settling tank designers, the feed-well mixing also playsan important role in the performance of the system.

For liquid-liquid separation, a large variety of chemical additives canbe applied depending on the properties and characteristics of aparticular liquid under test.

As noted above, the invention described herein comprises an automaticflocculating dosing device for each sedimentation cylinder, as animportant part of its structure, operation and method.

Identification of Additives and Dosage (Solid-Liquid Separation)

To identify the type of chemical additive to use in a solid-liquidseparation, there are various styles of tests performed on a laboratoryscale. The most common standard is a “jar-test” whereby a flask of knownvolume, containing slurry of a known solids mass and volume, is dosedwith a chemical additive and mixed, normally by hand, and then thesettling bed position is determined manually with a stopwatch and visualheight reference, over a fixed period of time. The methodology toperform the test is an international standard as documented in theAmerican Society for Testing Materials Norm ASTM D-2035. Data from thetest is commonly interpreted using various methods, primarily the Kynchand Coe-Clevenger methods, which rely on the accuracy of the datacollection to identify the optimum parameters of the chemical additivesto be used in the full scale process operation.

The “jar-test” is considered a static settling test whereby the settledmud (underflow) and the liquor (overflow) are not removed during thetest. It is becoming increasingly common that these static tests areused to identify the parameters to be verified with further small scaledynamic tests before implementation on a larger scale. These dynamictests were developed to improve the prediction of the unit area definedby the static test, for the thickener, clarifier and settling tank aspart of the design process.

Technology exists that can help to improve the “jar-test”, concepts ofwhich are discussed as per an optical device for monitoring the clarityof fluids as presented in U.S. Pat. No. 2,411,092 and later in U.S. Pat.No. 3,954,342 whereby the use of a light emitter and photodiode orreceptor are disclosed to measure the clarity of fluids and display aunit of measurement on a readout. This type of technology is the commonconcept for turbidimeters and has since been modified over recent yearsto include light scattering sensors to improve its accuracy.

U.S. Pat. No. 4,976,871 teaches the use of an inline constant flowmeasurement of slurry using a light source and a photocell to be able tocontrol flocculation dosing. This is a dynamic test that is used as aconstant measuring device to identify the solids concentration of a flowof slurry in a stream.

U.S. Pat. No. 5,431,037 documents an inline control device consisting ofa settling chamber that is installed adjacent to a thickener whereby asample of overflow water from the thickener is drawn into a settlingchamber to analyse the settling characteristics of the material andcontrol the rate of addition of the flocculant to the thickener by theflocculant supply device, and therefore prevent excessive amounts offlocculant or increase the dosage depending on the clarity of theoverflow water. The control device is designed for a continual operationto effectively verify the operation of the thickener and better controlthe flocculant dosage. The settling chamber draws a sample from thethickener via vacuum into the chamber until the liquid reaches twoheight probes, whereby the vacuum valve is closed and a timer starts. Asthe particulates in the liquid sample settle, a single light beam fixedto one side of the chamber then strikes a single photoelectric cell onthe opposite side which stops the timer for a certain reading. Theelectronic control circuit uses this time in an algorithm to produce anoutput signal to control the flocculant addition to the thickener. Thechamber empties, is washed by an input valve and the processautomatically repeated as part of the continual operation of thethickener. The light source and photocell are used to determine anacceptable clarity of water based on the drawn overflow water obtainedfrom the thickener to control the flocculant dosing and improve theclarity of the overflow water recovered from the thickener. The lightsource and photocell are not used to measure the settling velocity of aslurry or pulp, how this changes with time, the clarity of the waterover different heights within the chamber during the settling test, afinal mud bed depth and volume after a specific time nor produce datafor interpretation of solid-liquid settling rates for sizing athickener, clarifier or settling tank.

The previous described patent is based on almost the same principal as aprior art documented in U.S. Pat. No. 4,318,296 where a singlephotodiode and photocell are used in a settling cylinder to measurefixed position clarity of a liquid and thereby control the flocculationdelivery within a settling tank.

U.S. Pat. No. 4,779,462 documents an apparatus for automaticallymeasuring the apparent density of a mud or sludge contained in a liquidand the automatic measurement of the Ponsar Index. As part of theapparatus, a cylinder is used that is filled with 1.5 liters ofclarified liquid that is then filled with 1 liter of mud containingwater that is allowed to settle for a period of 30 minutes which isrequired to determine a parameter associated with the calculation of thePonsar Index. A stepper motor controls a single or series of photodiodesand a single photocell that is located on the opposite side of thecylinder. The stepper motor moves the photodiodes and photocell up anddown the cylinder to identify the position of the settled mud bed afterthe 30 minute period of time, and with the number of steps made by themotor, the apparatus can calculate the height and therefore the volumeof settled mud over this fixed time period.

The photodiodes and photocell only calculate the volume of mud after the30 minute period to report the volume parameter of the mud as part ofthe calculations of the entire operation of the apparatus. No real-timesettling rate behaviour of the slurry and the use of chemical additivesare considered. One of the inventors of this patent was granted U.S.Pat. No. 4,830,126 which is a modified apparatus to determine the PonsarIndex, and includes the same said settling cylinder, but considering ascrew device to move the photodiodes and photocell after the 30 minuteperiod.

Automatic control and optimized operation of the static “jar-test” styleof measurement of solid-liquid separation of slurries has been acontinuing concern of chemical additive vendors as well as settlingequipment manufactures. The “jar-test” was first standardised by ASTM in1999 to reduce result variability and define a test methodology.

However, no alternative standard currently exists. This is the subjectof the current invention and the goal of the inventors, transform theway of performing tests by using a method of data collection thatreduces errors and which through a program, delivers results, data orparameters digitized. Therefore, the aforementioned invention can beapplied to provide precise, real-time control and monitoring of suchsettling tests to meet industrial needs as well as the possibility tostandardise this type of test.

SUMMARY OF INVENTION

1. Objectives

-   -   Transform the way in which solid-liquid or liquid-liquid        sedimentation tests are done in order to reduce human error and        increase the frequency, precision and accuracy of the data by an        apparatus and method that using a custom programmation generates        immediate, computerized and reliable results.    -   Allow the simultaneous testing and data collection of multiple        samples, considering the same standardised operating conditions        and test parameters.    -   Reduce the labour intensity associated with the prior art to        allow more tests to be performed under different additives,        dosages, dilutions and densities, thereby producing more test        data in a given time frame.    -   Allow a third party to remotely access and interpret the data        from the settling tests by applying custom models, together with        (but not limited to) known models such as the Kynch and        Coe-Clevenger models for solid-liquid separation, for        comparative analysis and reporting.    -   Optimisation of thickeners, clarifiers, settling tanks and        similar equipment including the operating conditions, chemical        reagent dosages, and slurry or liquid chemistry used for        industrial phase separation processes, including but not limited        to the improvement of clarity of recovered liquor, reduction of        additive dosages and consumptions costs, and the reduction of        slurry or density specific liquid contamination.        2. Technical Problem

Perform various sedimentation tests under the same conditions and with amethodology for electronic characterization of the behaviour ofsedimentation.

Solution to Problem

The concerns or limitations regarding the prior art of static settlingtests (principally the “jar-test” for solid-liquid separation) areovercome with the presented invention that transforms data collection bya method that removes manual interaction and measurement, allowing teststo be run in parallel thus duplicating the same conditions, and allowingcomputational statistical analysis of the results both during and afterthe test is conducted.

The invention further allows multiple sedimentation cylinders to beinstalled (normally 12) located externally in a frame or structure thatrotates, mixing each sedimentation cylinder under the same mixingconditions. This is an automated mixing mechanism that ensures allfuture tests can be performed under the same mixing conditions. Eachsedimentation cylinder is fitted with a housing that incorporatesemitter and receiving sensors, which can be sensors to sense mud bedposition, final mud bed height, solids density, liquid density andclarity of the liquor. Receiving sensors are selected from the groupcomprising: photosensors, but can also be based on IR, UV, or opticalsensitivity depending on the wavelength of the emitter device. Emittersensors are selected from the group comprising: Light Emitting Diode(LED), IR, UV, laser or fixed/variable wavelength emitter.

Preferably, each housing is fitted with a minimum of four wavelengthemitting sensors and four wavelength receiving sensors, facing eachother and spaced at varying distances (depending on the type of thematerial under test) along the body of the housing, connected to acontrol system, to allow interpretation of the data successfully,although eight or more sensors are preferred, to allow highermeasurement precision of the mud bed position and/or consolidation overtime, or for liquid-liquid separation, the interfaces between twoliquids with different densities over time. The housing fits over acustom transparent sedimentation cylinder with stoppers where theslurry, pulp or liquids are contained during the mixing and settlingprocess. In addition, each housing has a chemical additives injectionsystem as flocculants that are part of the structure and are anessential part of the apparatus and method by directly influencingsedimentation and results delivered, unlike only sedimentation bygravity.

The sensors are non-intrusive, incorporated directly in the housingdesign, and are connected to a control system, which records informationof each sensor relative to the mud bed position, and/or herconsolidation within time or the interfaces between two liquids withdifferent densities. Furthermore, each sedimentation cylinder has theoption to have a sensor installed within the slurry to measure the pH,temperature, oxidation reduction potential, and conductivity dependingon the requirements of the test.

The control system collects and interprets data delivered by sensors;further it provides the status of the sensors during sedimentationtests. Moreover also communicates, processes, records and stores datafrom sensors in real time.

The control system, preferably but not limited to a small and portableLinux operating system, is coded with custom software, developed as partof the invention. The operating system is self-contained and connectedto a screen or touchscreen, with input devices as preferred by the user(commonly an optical device and keyboard).

The control system and said custom software are designed to receive allsensor outputs at predetermined time intervals. These time intervals maybe shorter during the first few minutes from the start of the settlingtests and increase with time as required. The data is generated inreal-time, stored locally, transmitted to a remote computer or serverand subsequently used to provide feedback to the user prior to, duringand after the settling test process. Using the data inputs from thesensors described as part of the invention, various analysis techniquesare performed, including but not limited to signal processing,statistical analysis, rule-based processing including fuzzy, discrete,or heuristic logic, data management, pattern and series recognition,categorical analysis, or a combination thereof. The software of thecontrol system can be modified or varied based on user input and subjectto any preferred analytical method to be implemented.

The control system activates various control devices during operation,including but not limited to the mixing of the slurry or liquids withinthe tubes; the injection of chemical additives, flocculants orcoagulants; sensor control; interaction with a Human Machine Interface(HMI); and the storage, transmission and reception of data andinformation.

The HMI is to allow information regarding the origins andphysico-chemical properties of the slurry, information related to thetype and quantity of each chemical additive, feedback to the user on thecurrent status of the test, error detection and/or alarming, tubereadiness and/or test completion, and data integrity and/or storage.

3. Advantageous Effects of the Invention

The method and apparatus are principally designed for solid-liquidseparation of laboratory through to pilot scale testing of slurries andpulps to identify operational parameters for full scale thickeners,clarifiers and settling tank equipment. The advantageous effects of theinvention are the transformation in the data collection and hence theaccuracy is improved, by reducing test errors through removing manualinteraction. This allows for a better comparison of data between testsperformed on the same pulps while varying the characteristics of theadditives used. This could engender the following advantages to theglobal solid-liquid separation field:

-   -   Optimization of selection of additive type, dose and        preparation.    -   Optimization of recovery and clarity of liquor through correct        additive selection and operational parameter identification.    -   Reduction of additive consumption and cost.    -   Reduction of slurry or pulp contamination through excess dosing.    -   Improvement of accuracy and precision of rheological testing of        the settled solids.    -   Possibility of having accurate data/results in real time and        accessed remotely.    -   Removal of manual errors in data collection

BRIEF DESCRIPTION OF THE DRAWINGS

FIG. 1 presents the current prototype of 12 sedimentation cylindersdesigned for laboratory scale use, that was considered for thedevelopment of the control system and optimum sensor position. Therotational motor and rotational housing are not shown.

FIG. 2 presents the concept of the functionality of a singlenon-intrusive emitter and receiving sensor array mounted in a singlesedimentation cylinder.

FIG. 3 presents a complete housing of the sedimentation cylinder usedwith 8 emitter and 8 receiving sensors.

FIG. 4 presents the bottom sedimentation cylinder stopper layout tocontain the settled slurry to facilitate removal of the solids portionfollowing completion of the solid-liquid settling test.

FIG. 5 presents the top sedimentation cylinder stopper layout for anelectronic additive injection.

DETAILED DESCRIPTION OF THE INVENTION

The invention relates to an apparatus for static sedimentation testscomprising a plurality of sedimentation cylinders, which are subject tothe same mixing conditions, said apparatus comprises:

a. A variable number of sedimentation cylinders, the most common being12 transparent sedimentation cylinders;

b. Each sedimentation cylinder is located inside a non-intrusive emitterand receiving sensor housing where each housing has an electronic IDcard, electronic circuit boards and connection to a control system;

c. A support structure containing the sedimentation cylinders and sensorhousings which rotates around an axis of rotation;

d. Each sedimentation cylinder has a bottom stopper and top stopper;

e. Where each bottom stopper of each sedimentation cylinder is mountedon a lateral bar parallel to the rotation axis, by a fixing to thesupporting structure;

f. Also the sedimentation cylinders are fixed in the supportingstructure by a clamping system around the top stopper of eachsedimentation cylinder;

g. The top stopper of each sedimentation cylinder has an additiveinjection system.

Also, there is a method for static sedimentation tests, carried out atthe same time and under the same mixing conditions in a plurality ofsedimentation cylinders, comprising:

(i) Add a solution which sedimentation tests generally require to beperformed on a variable number of sedimentation cylinders, the mostcommon being at least 12 transparent sedimentation cylinders, where eachsedimentation cylinder is located inside a non-intrusive emitter andreceiving sensor housing that is supported in a support structure whichrotates around an axis of rotation and each sedimentation cylinder has abottom stopper and top stopper, where the top stopper has an additiveinjection system;(ii) Rotate the sedimentation cylinders around an axis of rotation tohomogenise the solutions in each sedimentation cylinder;(iii) Stop the sedimentation cylinders in an upright position and addchemical additives to each sedimentation cylinder, through the additiveinjection system;(iv) Rotate again the sedimentation cylinders around the axis ofrotation, for mixing the solutions and additives;(v) Stop the sedimentation cylinders in an upright position;(vi) Start the sedimentation test;where all data from sedimentation tests and data delivered by eachnon-intrusive sensors with respect to mud bed position and/orconsolidation time, final mud bed height, solids density, liquid densityor clarity of the liquor are recorded by a control system.

Exemplary embodiments of the present invention are demonstratedhereinafter with reference to the accompanying figures.

Referring to FIG. 1, a sedimentation apparatus housing 12 sedimentationcylinders is presented. The number of sedimentation cylinders, theirdimensions and order of placement within the mixing apparatus can varyfrom the figure presented. The sedimentation cylinders presented in FIG.1 do not show the sensors; those are presented in FIGS. 2 and 3 in moredetail. The sedimentation cylinders and their sensor housing may beindependently installed within the apparatus. Also not shown in FIG. 1is the system to mix and rotate the apparatus. The rotation is madearound an axis (1) whereby the support structure (2) can rotate 360degrees if required, depending on the mixing operation required. Eachsedimentation cylinder has a bottom stopper (3) and top stopper (4)where the bottom stopper (3) is mounted on a lateral bar by a fixing (5)to the supporting structure (2). The sedimentation cylinder is fixed inthe supporting structure (2) by a clamping system (6) around the topstopper (4) whereby, but not limited to, two sedimentation cylinders canbe mounted together. The top stopper (4) of each sedimentation cylinderhas an additive injection system (7) that varies depending on the typeand quantity of additive to be used, however, FIG. 5 presents a moregeneric electronic stopper system developed as part of the invention.

Using the control system, each sensor housing has an electronicidentification tag so that the data can be logged from a specificsedimentation cylinder and be identified in the data. Prior to the startof the test, the control system requests that the user provide datarelating to the properties of the material, origin and test parametersto be used for the test. The control system also checks that the sensorsare operating correctly and the housings are correctly attached prior tothe mixing stage.

The clamped structure is rotated around an axis controlled by thecontrol system. The gyration sequence used can be modified as part ofthe control system. The mixing sequence is performed in a two stageprocess, firstly to ensure the pulp in the sedimentation cylinders isthoroughly mixed. The apparatus then stops at its vertical position andthe chemical additives are added into the sedimentation cylinders. Theuser triggers the start of the second stage of mixing whereby theapparatus rotates and mixes the pulp and additives. The apparatus thenstops at its vertical position and the settling test formally commences.

The displacement of the settling material is generally at its highest atthe beginning of a test; hence the control system allows for the datacollection frequency to be variable and therefore to allow for a higherfrequency data sampling rate as required. The data collection frequencycan be modified by the control system both locally or remotely asrequired.

FIG. 2 presents the concept of the functionality of a singlenon-intrusive emitter (8) and receiving sensor array (9) mounted on thehousing (C) of a single sedimentation cylinder for a solid-liquidsettling scenario. The emitter sensor (8) transmits a fixed wavelengthor variable wavelength that is received and processed by the receivingsensor (9). If the mud bed (10) is above the sensor position acalibrated reading is generated, and as the bed passes the receivingsensor the time is recorded and the wavelength intensity continuouslymonitored to establish the clarity of the liquor above the moving bedwith time. Each sensor along the housing records the same information ina simultaneous form controlled by the control device to determine thesettling bed position with time, the clarity of the liquor (11) atvarious depths above the moving bed, and the final settled mud bedheight (12). The test normally runs for a period of 24 hours but can bemodified by the control system both locally or remotely when required torun for different periods of time. The sedimentation cylinder wall (13)and internal wall (14) of the housing (C) are shown and preferable incontact. For liquid-liquid settling tests, the most dense liquid, orintermediate boundaries can be determined as they pass each sensorlocation.

FIG. 3 presents a housing (C) of a complete sedimentation cylinder, usedwith 8 emitter (15) and 8 receiving sensors (16) installed. The numberand position varies depending on the sedimentation cylinder to be usedand the type of material requiring testing. The housing (C) fits overthe sedimentation cylinder containing the pulp and rests on the bottomstopper as shown in FIG. 4. Each housing (C) contains the sensors,electronic circuit boards, associated wiring, and the data connection tothe main control system. Once positioned in the sedimentation apparatus,the housing and sedimentation cylinder with top and bottom stoppers isclamped into the apparatus. The top stopper, as shown in FIG. 5 with anelectronic additive injection system, is used to contain the chemicaladditive, if required as part of the test. The additive is prepared andmeasured accordingly to be pre-installed in the injection system whichis either activated by the user manually or automatically by the controlsystem prior to the second stage of mixing. This top stopper andinjection system is designed to allow the pulp and liquor contained inthe sedimentation cylinder to wash all remnants of the additive from thecontainer during the second stage of mixing, so as to ensure the entireadditive has entered the pulp.

FIG. 4 shows the position of a final mud bed or dense liquid interface(17), the position of which varies depending on the characteristics ofthe solid-liquid or liquid-liquid mixture. The bottom stopper (18) ispreferably made of natural rubber that can be removed from thesedimentation cylinder by the user. The height and width of the stoppervary depending on the sedimentation cylinder to be used and the type ofmaterial required for testing. The final sensor position (19) on thehousing (C) varies depending on the type of solid-liquid orliquid-liquid mixture to be used. The liquor or liquid of lesser density(20) is contained in the sedimentation cylinder above the mud bed orliquid of higher density (17).

FIG. 5 shows the top stopper (20) with a generic additive injectionsystem (21), which can be an electronic injection system comprising anelectronic valve (22) permitting the additive to feed the sedimentationcylinder either by gravity or pressure. The height and width of thestopper vary, so as the injection system, depending on the sedimentationcylinder to be used, the type of material that requires testing, andchemical additive dosage required. The valve has to be 2 way to allowthe backward flow of slurry or liquid to wash back into the additivecontainer to ensure that all additive injection has entered thesedimentation cylinder (23). A support system (24) for the valve andadditive container ensures that both said items can be removed with therubber stopper (20).

The wires (25) can be disconnected from the control system, whichcontrols the additive injection system. The electronic valve cancorrespond to a solenoid valve preferably a pressure valve which iscontrolled by the control system.

An alternative to the electronic injection system as shown in FIG. 5 isa manual injection system of quick release by button release or syringestyle applications. This is operated by the user prior to the secondmixing stage and start of the settling test. The electronic system ispreferred to improve the accuracy of the additive injection by allowingfor the simultaneous operation of each sedimentation cylinder.

The emitter sensors are all powered by a common rail that is fed fromthe same power source as the control system.

The control system, as per present day technology but not limited to, iscurrently based on a Linux operating system and is a self-containedequipment that accompanies the apparatus and is operated by the HMI, andinput devices as preferred by the user (optical device and keyboard).The computer, when connected to the internet by cable or wireless, canbe remotely accessed to perform a variety of tasks including, but notlimited to, diagnosing in real time the sedimentation test throughsensors, accessing and manipulating stored test data results, modifyingsedimentation cylinder identification data and changing remotecommunication and data upload parameters. The system is designed toprocess and upload or distribute the data electronically to a thirdparty user or server for further analysis and processing. The user orclient then receives the presentation of the interpreted data viaelectronic means or remote server access.

The control system may incorporate connections to log data fromadditional intrusive sensors installed in each sedimentation cylinder.These sensors may measure, in parallel with the housing sensors, otherslurry properties including but not limited to, pH, temperature,oxidation reduction potential, and conductivity. These sensors each havean electronic identification to allow the computer to record thesedimentation cylinder location and group its data with thecorresponding receiving sensors.

At the end of the test, the sensor housing and contained sedimentationcylinders are unclamped and carefully removed from the apparatus. Thehousing is removed and the liquor from each sedimentation cylinder canbe extracted to leave the solids at the base of the sedimentationcylinder. The bottom stopper is carefully removed to access the solidsfor further testing such as, rheology, particle size distribution,specific gravity, plasticity limits, and any other mineral or liquidcharacterization techniques.

Due to modern advances in technology, it is envisaged that the samesensor control, data collection and processing methods can be integratedon more compact, reliable technology platforms so as to improve theoperation of the apparatus in the future.

The invention claimed is:
 1. Apparatus for static sedimentation testscomprising a plurality of sedimentation cylinders, which are subject tothe same mixing conditions, said apparatus comprises: a. A plurality oftransparent sedimentation cylinders; b. Each sedimentation cylinder islocated inside a non-intrusive emitter and receiving sensor housingwhere each housing has an electronic ID card, electronic circuit boardsand connection to a control system; c. A support structure containingthe sedimentation cylinders and sensor housings which rotates around anaxis of rotation; d. Each sedimentation cylinder has a bottom stopperand top stopper; e. Where each bottom stopper of each sedimentationcylinder is mounted on a lateral bar parallel to the rotation axis, by afixing to the supporting structure; f. Also the sedimentation cylindersare fixed in the supporting structure by a clamping system around thetop stopper of each sedimentation cylinder; g. The top stopper of eachsedimentation cylinder has an additive injection system.
 2. Apparatusaccording to claim 1, wherein the additive injection system is a quickrelease injection system that can be activated manually or by thecontrol system.
 3. Apparatus according to claim 2, wherein said sensorsare sensors to sense mud bed position, final mud bed height, solidsdensity, liquid density and clarity of the liquor.
 4. Apparatusaccording to claim 3, wherein said non-intrusive receiving sensors areselected from the group comprising photosensors, IR, UV, optical orwavelength based sensitivity sensors and said non-intrusive emittingsensors are selected from the group comprising, Light Emitting Diode(LED), IR, UV, laser or fixed/variable wavelength emitter.
 5. Apparatusaccording to claim 4, wherein each housing is equipped with at least 4emission wavelength sensors and with at least 4 reception wavelengthsensors, facing each other and spaced at varying distances (depending onthe type of the material under test) along the housing body. 6.Apparatus according to claim 5, wherein the sensors of each housing areconnected to a control system, which records information of each sensorrelative to the mud bed position and/or consolidation over time or theinterfaces between two liquids with different densities.
 7. Apparatusaccording to claim 6, wherein in addition, each sedimentation cylinderhas at least a sensor installed within the slurry (intrusive sensors) tomeasure at least one of the group consisting of pH, temperature,oxidation reduction potential, conductivity of the suspension that issubjected to the sedimentation tests, and combinations thereof, whosedata is recorded in parallel to data of the non-intrusive sensors by thecontrol system.
 8. Apparatus according to claim 7, wherein the housingswith their sedimentation cylinders are located outwardly of the supportstructure and the sedimentation cylinder wall and internal wall of thehousing are in contact.
 9. Apparatus according to claim 8, wherein theclamping system around the top stopper, mount together two sedimentationcylinders to the rotational axis.
 10. Apparatus according to claim 9,wherein the housing of each sedimentation cylinder rests on the bottomstopper of the sedimentation cylinder, stopper which is made of naturalrubber and can be easily removed from the sedimentation cylinder, afterthe sedimentation test, to easily access the settled solids. 11.Apparatus according to claim 10, wherein the control system is connectedto intrusive and non-intrusive sensors and collects and interprets datadelivered by sensors; further provides the status of the sensors, thecontrol system also communicates, processes, records and stores datafrom sensors in real time.
 12. Apparatus according to claim 11, whereinthe control system also provides real-time diagnostics through sensorsof the sedimentation tests, and upload or distributes the data to astorage media, a computer or a server, wherein the diagnosis of thecontrol system consists in inform whether the connection of the sensorsis correct, if the operation of the sedimentation cylinders is corrector the status of each sedimentation cylinder during the sedimentationtest.
 13. Apparatus according to claim 12, wherein the control system isalso connected to a remote server or data storage system via theinternet by cable or wireless communication whereby the data collectedby the sensors is evaluated and processed remotely on a third partyserver and then results are sent via electronic form or by remote serveraccess by the user.
 14. Apparatus according to claim 12, wherein thecontrol system is also connected and controlled by a Human MachineInterface (HMI) to allow initial data regarding the physicochemicalproperties of the slurry from the sedimentation test and chemicaladditive contained in each sedimentation cylinder are registered, wherethe HMI also controls the operation of the sedimentation test. 15.Apparatus according to claim 1, wherein the plurality of transparentsedimentation cylinders is
 12. 16. Method for static sedimentation testscarried out simultaneously and under the same mixing conditions in aplurality of sedimentation cylinders, said method comprises: (i) Add asolution which sedimentation tests are required to be performed to aplurality of transparent sedimentation cylinders, where eachsedimentation cylinder is located inside a non-intrusive emitter andreceiving sensor housing, where the sensor housings are supported in asupport structure which rotates around an axis of rotation and eachsedimentation cylinder has a bottom stopper and top stopper, where thetop stopper has an additive injection system; (i) Rotate thesedimentation cylinders around an axis of rotation to homogenise thesolutions in each sedimentation cylinder; (ii) Stop upright thesedimentation cylinders and add chemical additives to each sedimentationcylinder, (iii) Rotate again the sedimentation cylinders around the axisof rotation, for mixing the solutions and additives; (iv) Stop uprightthe sedimentation cylinders; (v) Start the sedimentation test; where alldata from sedimentation tests and data delivered by each non-intrusivesensors with respect to mud bed position and/or consolidation time,final mud bed height, solids density, liquid density or clarity of theliquor are recorded by a control system.
 17. Method according to claim16, wherein the plurality of sedimentation cylinders is 12 and also haveintrusive sensors and the method also includes measurement of pH,temperature, oxidation reduction potential, and conductivity of thesuspension of those sensors whose data is recorded in parallel to dataof the non-intrusive sensors by the control system.
 18. Method accordingto claim 17, wherein at the end of the sedimentation tests, the sensorhousing and contained sedimentation cylinders are unclamped and removedfrom the support structure, the top stopper is removed to access theliquor from each sedimentation cylinder leaving the solids at the baseof each sedimentation cylinder, the bottom stopper is removed so thesolids can be extracted for further tests.
 19. Method according to claim18, wherein the further tests are selected from at least one ofrheology, particle size distribution, specific gravity, plasticitylimits, or liquid or characterization techniques of mineral or liquid.20. Method according to claim 19, wherein the control system cancommunicate, process, interpret, diagnose, record and store data fromintrusive and non-intrusive sensors, in real time, distributing the dataelectronically to a computer or server, that may be a remote server. 21.Method according to claim 20, wherein the control system diagnoseswhether the connection of the sensors is correct, if the operation ofthe sedimentation cylinders is correct or the status of eachsedimentation cylinder during the sedimentation test.
 22. Methodaccording to claim 21, wherein the data collected by the sensors isevaluated and processed remotely on a third party server by sending viaelectronic form or by remote server access by the user wherein theremote server is connected to the control system via the internet bycable or wireless communication.
 23. Method according to claim 22,wherein said control system is connected and controlled by a HumanMachine Interface (HMI) to allow initial data being registered regardingthe physicochemical properties of the slurry from the sedimentation testand the chemical additive to be used.